NMR Experiments and Sequences
Triple Resonance Experiments for Side-chain Assignments

Bruker Abbriviations; tr (TROSY), gp (Gradient Pulse), dipsi (DIPSI sequenc), mlev (MLEV sequenc), si (Sensitivity Increase), et (Echo-Antiecho Coherence Selection)
NMR Experiments Bruker Sequences
(H)CC(CO)NH
with CC-TOCSY
hccconhgp3d3
Acquires 3D; F3(HN) - F2(N) - F1(C)
trhccconhgp3d3
H(CC-CO)NH
with CC-TOCSY
hccconhgp3d2
Acquires 3D; F3(HN) - F2(N) - F1(HC)
trhccconhgp3d2
(H)CCH-TOCSY
with CC-TOCSY
hcchdigp3d2
Acquires 3D; F3(HC) - F2(C) - F1(C)
H(C)CH-TOCSY
with CC-TOCSY
hcchdigp3d
Acquires 3D; F3(HC) - F2(C) - F1(HC)
(H)CCH-COSY
with CC-COSY
hcchcogp3d2
Acquires 3D; F3(HC) - F2(C) - F1(C)
H(C)CH-COSY
with CC-COSY
hcchcogp3d
Acquires 3D; F3(HC) - F2(C) - F1(HC)
TOCSY-15N-HSQC
with HH-TOCSY
dipsihsqcf3gpsi3d
Acquires 3D; F3(HN) - F2(N) - F1(H)
dipsitretf3gp3d; TROSY vrsion
TOCSY-13C-HSQC
with HH-TOCSY
mlevhsqcetgp3d
Acquires 3D; F3(HC) - F2(C) - F1(H)

Experiments Connecting Backbone and Sidechain Assignments



Experiment for Sidechain Assignments